Combined EDS and EBSD dataset from TiB2 ceramic material

10.13139/ORNLNCCS/1819695

This is supplemental information to a paper to be submitted, tentatively titled Cluster analysis of combined EDS and EBSD data to solve ambiguous phase identifications. Data was acquired from a TiB2 ceramic provided by Missouri University of Science and Technology. Simultaneous EDS and EBSD were acquired on a Tescan MIRA3 GMH field-emission SEM equipped with Oxford Instruments Symmetry CMOS-based EBSD detector and Oxford Instruments UltimMax 170 mm2 silicon-drift detector EDS. Data was acquired using Oxford Instruments AZtec 4.0 software. Data was acquired at 20 keV, 70° tilt, and ≈1 nA probe current. An 80×60 pixel, 40×30 μm map (500 nm pixel pitch) was acquired. EBSD indexing was performed using TiB2, space group 191 P6/mmm, and TiC, space group 225 Fm \bar{3}m, crystal cards.

Published: 2021-09-21 09:07:17 Download Dataset

Dataset Properties

Field Value
Authors
  • Parish, Chad Oak Ridge National Laboratory
Project Identifier EDS and EBSD analysis
Dataset Type ND Numeric Data
Subjects
  • 36 MATERIALS SCIENCE
Keywords
  • EDS
  • EBSD
  • SEM
Originating Organizations Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organizations Office of Science (SC)
DOE Contract DE-AC05-00OR2272

Acknowledgements

Papers using this dataset are requested to include the following text in their acknowledgements:

*Support for 10.13139/ORNLNCCS/1819695 is provided by the U.S. Department of Energy, project EDS and EBSD analysis under Contract DE-AC05-00OR2272. This research used resources of the Oak Ridge Leadership Computing Facility, which is a DOE Office of Science User Facility.