Combined EDS and EBSD dataset from TiB2 ceramic material
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Chad Parish | Oak Ridge National Laboratory
Description
This is supplemental information to a paper to be submitted, tentatively titled Cluster analysis of combined EDS and EBSD data to solve ambiguous phase identifications. Data was acquired from a TiB2 ceramic provided by Missouri University of Science and Technology. Simultaneous EDS and EBSD were acquired on a Tescan MIRA3 GMH field-emission SEM equipped with Oxford Instruments Symmetry CMOS-based EBSD detector and Oxford Instruments UltimMax 170 mm2 silicon-drift detector EDS. Data was acquired using Oxford Instruments AZtec 4.0 software. Data was acquired at 20 keV, 70° tilt, and ≈1 nA probe current. An 80×60 pixel, 40×30 μm map (500 nm pixel pitch) was acquired. EBSD indexing was performed using TiB2, space group 191 P6/mmm, and TiC, space group 225 Fm \bar{3}m, crystal cards.
Funding Information
DOE Contract Number
DE-AC05-00OR22725Originating Research Organization
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)Sponsoring Organization
Office of Science (SC)Details
Release Date
September 21, 2021Subject
36 MATERIALS SCIENCEKeywords
EDS, EBSD, SEMDataset
Dataset Type
ND Numeric DataCite This Dataset:
Parish, C. (2021). Combined EDS and EBSD dataset from TiB2 ceramic material. Oak Ridge National Laboratory. https://doi.org/10.13139/ORNLNCCS/1819695.
Acknowledgements
This work was carried out [in part] at Oak Ridge National Laboratory, managed by UT-Battelle, LLC for the U.S. Department of Energy under contract DE-AC05-00OR22725.